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表面電離検出ガスクロマトグラフィーの法中毒学的応用
http://hdl.handle.net/10271/1681
http://hdl.handle.net/10271/16819a00d404-cb11-4173-a54d-0e55d88c54f8
名前 / ファイル | ライセンス | アクション |
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FT-10-82.pdf (102.1 kB)
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Item type | 学術雑誌論文 / Journal Article(1) | |||||
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公開日 | 2013-08-27 | |||||
タイトル | ||||||
言語 | ja | |||||
タイトル | 表面電離検出ガスクロマトグラフィーの法中毒学的応用 | |||||
言語 | ||||||
言語 | jpn | |||||
資源タイプ | ||||||
資源タイプ識別子 | http://purl.org/coar/resource_type/c_6501 | |||||
資源タイプ | journal article | |||||
その他のタイトル | ||||||
その他のタイトル | APPLICATION OF GAS CHROMATOGRAPHY-SURFACE IONIZATION DETECTION TO FORENSIC TOXICOLOGY | |||||
言語 | en | |||||
著者 |
妹尾, 洋
× 妹尾, 洋× 服部, 秀樹× 熊澤, 武志× 鈴木, 修× 木村, 美智子× 山田, 高路 |
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書誌情報 |
ja : 法中毒 = Japanese journal of forensic toxicology 巻 10, 号 2, p. 82-83, 発行日 1992-09-30 |
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出版者 | ||||||
言語 | ja | |||||
出版者 | 日本法中毒学会 | |||||
権利 | ||||||
言語 | ja | |||||
権利情報 | Copyright 日本法中毒学会 | |||||
権利 | ||||||
言語 | ja | |||||
権利情報 | 本文データは日本法中毒学会の許諾のもと掲載しています。 | |||||
抄録 | ||||||
内容記述タイプ | Abstract | |||||
内容記述 | Tricyclic antidepressants and local anesthetics were detected by gas chromatography (GC)-surface ionization detection (SID), which has been reported to be very sensitive and specific to tertiary amines. The detection limit in an injected volume was 5-10 pg for amitriptyline, imipramine, trimipramine, chlorimipramine, lidocaine, mepivacaine and bupivacaine, and 100-200 pg for procaine, benoxinate and dibucaine. When compared with the GC-nitrogen-phosphorus detection (NPD), the GC-SID sensitivity was 10-100 times higher, the background was cleaner, and the baseline remained steady as the column temperature was increased. The drugs could bee rapidly isolated with Sep-Pak C18 cartridges from biological fluids before GC. The recovery of the drugs was more than 60%. | |||||
言語 | en | |||||
ISSN | ||||||
収録物識別子タイプ | ISSN | |||||
収録物識別子 | 09159606 | |||||
著者版フラグ | ||||||
出版タイプ | VoR | |||||
出版タイプResource | http://purl.org/coar/version/c_970fb48d4fbd8a85 |