@article{oai:hama-med.repo.nii.ac.jp:00001658,
 author = {李, 暁鵬 and 熊澤, 武志 and 佐藤, 啓造 and 鈴木, 修},
 issue = {2},
 journal = {法中毒 = Japanese journal of forensic toxicology},
 month = {May},
 note = {A simple and rapid method, for the extraction of four diazine herbicides (terbacil, bromacil, norflurazon and PAC) from human whole blood, plasma and urine, using Bond-Elut C18 cartridges, is presented. After mixing with distilled water, whole blood, plasma and urine samples containing the herbicides were loaded on Bond-Elut C18 cartridges and eluted with chloroform/methanol(9:1). The herbicides were detected by capillary gas chromatography with flame ionization detection (FlD) with splitless injection. Separation of four diazine herbicides from each other and from impurities was generally satisfactory with the use of an intermediately polar DB-17 capillary column. The recovery of these compounds was more than 90%. The calibration curve for the four herbicides, which had been added to whole blood, plasma and urine, showed linearity in the range of 1.6-100 ng on column. The detection limits of the herbicides were about 1.2-1.4 ng on column.},
 pages = {118--119},
 title = {ダイアジン系除草剤の固相抽出法とキャピラリーガスクロマトグラフィー},
 volume = {12},
 year = {1994}
}