{"created":"2023-06-20T15:47:07.488255+00:00","id":1663,"links":{},"metadata":{"_buckets":{"deposit":"20f8f8bf-d24d-4281-a700-35301856dd8a"},"_deposit":{"created_by":4,"id":"1663","owners":[4],"pid":{"revision_id":0,"type":"depid","value":"1663"},"status":"published"},"_oai":{"id":"oai:hama-med.repo.nii.ac.jp:00001663","sets":["1:11"]},"author_link":["3736","3737","3738","3739","3740","3741"],"item_3_alternative_title_1":{"attribute_name":"その他のタイトル","attribute_value_mlt":[{"subitem_alternative_title":"三環系抗うつ剤のヘッドスペースSPMEによる簡易抽出法","subitem_alternative_title_language":"ja"}]},"item_3_biblio_info_5":{"attribute_name":"書誌情報","attribute_value_mlt":[{"bibliographicIssueDates":{"bibliographicIssueDate":"1995-04-15","bibliographicIssueDateType":"Issued"},"bibliographicIssueNumber":"1","bibliographicPageEnd":"30","bibliographicPageStart":"25","bibliographicVolumeNumber":"13","bibliographic_titles":[{"bibliographic_title":"法中毒","bibliographic_titleLang":"ja"},{"bibliographic_title":"Japanese journal of forensic toxicology","bibliographic_titleLang":"en"}]}]},"item_3_description_9":{"attribute_name":"抄録","attribute_value_mlt":[{"subitem_description":"A simple method, for the extraction of four tricyclic antidepressants from human urine, using the headspace solid-phase microextraction (SPME) is presented. After heating a vial containing urine sample and the drugs at 100℃ in the presence of NaOH solution, a polydimethylsiloxane-coated SPME fiber was exposed in the headspace of the vial to allow adsorption of the drugs. The fiber needle was then injected into a capillary gas chromatography (GC) port. The headspace SPME-GC gave intense peaks for each drugs; only a few small background noises appeared. Recovery of the four drugs with use of the headspace SPME-GC were 44-81 %. The calibration curves showed linearity in the range of 0.05-2μg/ml. The detection limits of each drugs were 24-38 ng/ml. The present results on the analysis of tricyclic antidepressants by headspace SPME suggest its applicability to a number of other solid drugs and poisons of middle-sized molecular weights in forensic toxicology .","subitem_description_language":"en","subitem_description_type":"Abstract"}]},"item_3_publisher_6":{"attribute_name":"出版者","attribute_value_mlt":[{"subitem_publisher":"日本法中毒学会","subitem_publisher_language":"ja"}]},"item_3_rights_7":{"attribute_name":"権利","attribute_value_mlt":[{"subitem_rights":"Copyright 日本法中毒学会","subitem_rights_language":"ja"},{"subitem_rights":"本文データは日本法中毒学会の許諾のもと掲載しています。","subitem_rights_language":"ja"}]},"item_3_source_id_19":{"attribute_name":"ISSN","attribute_value_mlt":[{"subitem_source_identifier":"09159606","subitem_source_identifier_type":"ISSN"}]},"item_3_version_type_32":{"attribute_name":"著者版フラグ","attribute_value_mlt":[{"subitem_version_resource":"http://purl.org/coar/version/c_970fb48d4fbd8a85","subitem_version_type":"VoR"}]},"item_creator":{"attribute_name":"著者","attribute_type":"creator","attribute_value_mlt":[{"creatorNames":[{"creatorName":"Kumazawa, Takeshi"}],"nameIdentifiers":[{"nameIdentifier":"3736","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"Lee, Xiao-Pen"}],"nameIdentifiers":[{"nameIdentifier":"3737","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"Tsai, Miin-Chang"}],"nameIdentifiers":[{"nameIdentifier":"3738","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"Seno, Hiroshi"}],"nameIdentifiers":[{"nameIdentifier":"3739","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"Ishii, Akira"}],"nameIdentifiers":[{"nameIdentifier":"3740","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"Sato, Keizo"}],"nameIdentifiers":[{"nameIdentifier":"3741","nameIdentifierScheme":"WEKO"}]}]},"item_files":{"attribute_name":"ファイル情報","attribute_type":"file","attribute_value_mlt":[{"accessrole":"open_date","date":[{"dateType":"Available","dateValue":"2018-08-27"}],"displaytype":"detail","filename":"FT-13-25.pdf","filesize":[{"value":"296.8 kB"}],"format":"application/pdf","licensetype":"license_note","mimetype":"application/pdf","url":{"label":"FT-13-25.pdf","url":"https://hama-med.repo.nii.ac.jp/record/1663/files/FT-13-25.pdf"},"version_id":"57bafe28-62fc-4c32-845d-28c009d9ed73"}]},"item_keyword":{"attribute_name":"キーワード","attribute_value_mlt":[{"subitem_subject":"Solid-phase microextraction (SPME)","subitem_subject_language":"en","subitem_subject_scheme":"Other"},{"subitem_subject":"Headspace method","subitem_subject_scheme":"Other"},{"subitem_subject":"Amitriptyline","subitem_subject_scheme":"Other"},{"subitem_subject":"Chlorimipramine","subitem_subject_scheme":"Other"},{"subitem_subject":"Imipramine","subitem_subject_scheme":"Other"},{"subitem_subject":"Trimipramine","subitem_subject_scheme":"Other"},{"subitem_subject":"Gas chromatography","subitem_subject_scheme":"Other"}]},"item_language":{"attribute_name":"言語","attribute_value_mlt":[{"subitem_language":"eng"}]},"item_resource_type":{"attribute_name":"資源タイプ","attribute_value_mlt":[{"resourcetype":"journal article","resourceuri":"http://purl.org/coar/resource_type/c_6501"}]},"item_title":"SIMPLE EXTRACTION OF TRICYCLIC ANTIDEPRESSANTS IN HUMAN URINE BY HEADSPACE SOLID-PHASE MICROEXTRACTION (SPME)","item_titles":{"attribute_name":"タイトル","attribute_value_mlt":[{"subitem_title":"SIMPLE EXTRACTION OF TRICYCLIC ANTIDEPRESSANTS IN HUMAN URINE BY HEADSPACE SOLID-PHASE MICROEXTRACTION (SPME)","subitem_title_language":"en"}]},"item_type_id":"3","owner":"4","path":["11"],"pubdate":{"attribute_name":"PubDate","attribute_value":"2013-08-27"},"publish_date":"2013-08-27","publish_status":"0","recid":"1663","relation_version_is_last":true,"title":["SIMPLE EXTRACTION OF TRICYCLIC ANTIDEPRESSANTS IN HUMAN URINE BY HEADSPACE SOLID-PHASE MICROEXTRACTION (SPME)"],"weko_creator_id":"4","weko_shared_id":-1},"updated":"2023-08-02T03:59:00.783711+00:00"}