{"created":"2023-06-20T15:47:07.534329+00:00","id":1664,"links":{},"metadata":{"_buckets":{"deposit":"9667ef82-f1a5-4e86-bb38-a7d2f9985ad6"},"_deposit":{"created_by":4,"id":"1664","owners":[4],"pid":{"revision_id":0,"type":"depid","value":"1664"},"status":"published"},"_oai":{"id":"oai:hama-med.repo.nii.ac.jp:00001664","sets":["1:11"]},"author_link":["3742","3743","3744","3745","3746"],"item_3_alternative_title_1":{"attribute_name":"その他のタイトル","attribute_value_mlt":[{"subitem_alternative_title":"SIMPLE EXTRACTION OF ORGANOPHOSPHATE PESTICIDES USING SOLID-PHASE MICROEXTRACTION (SPME) BEFORE CAPILLARY GAS CHROMATOGRAPHY","subitem_alternative_title_language":"en"}]},"item_3_biblio_info_5":{"attribute_name":"書誌情報","attribute_value_mlt":[{"bibliographicIssueDates":{"bibliographicIssueDate":"1995-05-15","bibliographicIssueDateType":"Issued"},"bibliographicIssueNumber":"2","bibliographicPageEnd":"123","bibliographicPageStart":"122","bibliographicVolumeNumber":"13","bibliographic_titles":[{"bibliographic_title":"法中毒","bibliographic_titleLang":"ja"},{"bibliographic_title":"Japanese journal of forensic toxicology","bibliographic_titleLang":"en"}]}]},"item_3_description_9":{"attribute_name":"抄録","attribute_value_mlt":[{"subitem_description":"A simple method, for extraction of 9 organophosphate pesticides from human whole blood and urine, using the headspace solid-phase microextraction (SPME) method is presented. After heating a vial containing the samples and the pesticides (IBP, methyl parathion, fenitrothion, malathion, fenthion, isoxathion, ethion, EPN and phosalone) at 100°C , a polydimethylsiloxane-coated SPME fiber was exposed to the headspace of the vial to allow adsorption of the pesticides before a capillary gas chromatography (GC) with nitrogenphosphorus detection. The headspace SPME-GC for whole blood and urine gave peaks for each pesticides. Recoveries of the 8 pesticides were 11-0.3% for whole blood; those of the 9 pesticides were 40-3.8% for urine. The detection limits of each pesticide were 2.2-100 ng/0.5ml for whole blood and 0.8-12 ng/0.5ml for urine. Reproducibility for headspace SPME-GC data were excellent for both body fluids.","subitem_description_language":"en","subitem_description_type":"Abstract"}]},"item_3_publisher_6":{"attribute_name":"出版者","attribute_value_mlt":[{"subitem_publisher":"日本法中毒学会","subitem_publisher_language":"ja"}]},"item_3_rights_7":{"attribute_name":"権利","attribute_value_mlt":[{"subitem_rights":"Copyright 日本法中毒学会","subitem_rights_language":"ja"},{"subitem_rights":"本文データは日本法中毒学会の許諾のもと掲載しています。","subitem_rights_language":"ja"}]},"item_3_source_id_19":{"attribute_name":"ISSN","attribute_value_mlt":[{"subitem_source_identifier":"09159606","subitem_source_identifier_type":"ISSN"}]},"item_3_version_type_32":{"attribute_name":"著者版フラグ","attribute_value_mlt":[{"subitem_version_resource":"http://purl.org/coar/version/c_970fb48d4fbd8a85","subitem_version_type":"VoR"}]},"item_creator":{"attribute_name":"著者","attribute_type":"creator","attribute_value_mlt":[{"creatorNames":[{"creatorName":"李, 暁鵬"}],"nameIdentifiers":[{"nameIdentifier":"3742","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"熊澤, 武志"}],"nameIdentifiers":[{"nameIdentifier":"3743","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"田口, 智子"}],"nameIdentifiers":[{"nameIdentifier":"3744","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"佐藤, 啓造"}],"nameIdentifiers":[{"nameIdentifier":"3745","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"鈴木, 修"}],"nameIdentifiers":[{"nameIdentifier":"3746","nameIdentifierScheme":"WEKO"}]}]},"item_files":{"attribute_name":"ファイル情報","attribute_type":"file","attribute_value_mlt":[{"accessrole":"open_date","date":[{"dateType":"Available","dateValue":"2018-08-27"}],"displaytype":"detail","filename":"FT-13-122.pdf","filesize":[{"value":"125.7 kB"}],"format":"application/pdf","licensetype":"license_note","mimetype":"application/pdf","url":{"label":"FT-13-122.pdf","url":"https://hama-med.repo.nii.ac.jp/record/1664/files/FT-13-122.pdf"},"version_id":"809db050-4d50-4cb9-963d-940924deaa60"}]},"item_language":{"attribute_name":"言語","attribute_value_mlt":[{"subitem_language":"jpn"}]},"item_resource_type":{"attribute_name":"資源タイプ","attribute_value_mlt":[{"resourcetype":"journal article","resourceuri":"http://purl.org/coar/resource_type/c_6501"}]},"item_title":"有機リン系農薬のSPME法による簡易抽出とキャピラリーガスクロマトグラフィー","item_titles":{"attribute_name":"タイトル","attribute_value_mlt":[{"subitem_title":"有機リン系農薬のSPME法による簡易抽出とキャピラリーガスクロマトグラフィー","subitem_title_language":"ja"}]},"item_type_id":"3","owner":"4","path":["11"],"pubdate":{"attribute_name":"PubDate","attribute_value":"2013-08-27"},"publish_date":"2013-08-27","publish_status":"0","recid":"1664","relation_version_is_last":true,"title":["有機リン系農薬のSPME法による簡易抽出とキャピラリーガスクロマトグラフィー"],"weko_creator_id":"4","weko_shared_id":-1},"updated":"2023-08-02T03:59:05.525810+00:00"}