@article{oai:hama-med.repo.nii.ac.jp:00001665,
 author = {熊澤, 武志 and 李, 暁鵬 and 佐藤, 啓造 and 妹尾, 洋 and 石井, 晃 and 鈴木, 修},
 issue = {2},
 journal = {法中毒, Japanese journal of forensic toxicology},
 month = {May},
 note = {Local anaesthetics have been found extractable by headspace solid-phase  microextraction (SPME), and the best conditions of their extraction from human blood samples have been investigated. After deproteinization with perchloric acid solution, the clear supernatants of human whole blood samples containing the drugs were heated in a vial at 100°C in the presence of NaOH solution plus (NH4)2SO4; and a polydimethylsiloxane-coated SPME fiber was exposed to the headspace of the vial to allow adsorption of the drugs before capillary gas chromatography with flame ionization detection. Although the recovery of the ten drugs from human whole blood was 11-0.4 %, the calibration curves for 9 drugs showed linearity in the range of 1-12μg/ml, with detection limits of 60-830 ng/ml.},
 pages = {142--143},
 title = {ヒト血中局所麻酔剤のヘッドスペース固相ミクロ抽出（SPME）とキャピラリーガスクロマトグラフィー},
 volume = {13},
 year = {1995}
}