{"created":"2023-06-20T15:47:07.729298+00:00","id":1668,"links":{},"metadata":{"_buckets":{"deposit":"db65a9cf-4321-41a4-94d1-7bc59a3df752"},"_deposit":{"created_by":4,"id":"1668","owners":[4],"pid":{"revision_id":0,"type":"depid","value":"1668"},"status":"published"},"_oai":{"id":"oai:hama-med.repo.nii.ac.jp:00001668","sets":["1:11"]},"author_link":["3765","3766","3767","3768","3769","3770"],"item_3_alternative_title_1":{"attribute_name":"その他のタイトル","attribute_value_mlt":[{"subitem_alternative_title":"ヘッドスペース固相ミクロ抽出/ガスクロマトグラフィーによるヒト血中及び尿中メペリジン（ペチジン）の検出","subitem_alternative_title_language":"ja"}]},"item_3_biblio_info_5":{"attribute_name":"書誌情報","attribute_value_mlt":[{"bibliographicIssueDates":{"bibliographicIssueDate":"1995-09-15","bibliographicIssueDateType":"Issued"},"bibliographicIssueNumber":"3","bibliographicPageEnd":"215","bibliographicPageStart":"211","bibliographicVolumeNumber":"13","bibliographic_titles":[{"bibliographic_title":"法中毒","bibliographic_titleLang":"ja"},{"bibliographic_title":"Japanese journal of forensic toxicology","bibliographic_titleLang":"en"}]}]},"item_3_description_9":{"attribute_name":"抄録","attribute_value_mlt":[{"subitem_description":"A simple extraction method is presented for meperidine (pethidine) in human whole blood and urine using headspace solid phase microextraction (SPME) with diphenylpyraline as internal standard (IS). Clear supernatant of whole blood after deproteinization, and untreated urine, containing meperidine and IS, were heated at 100°C in the presence of NaOH and NaCl in a vial with a silicone septum cap; and then an SPME fiber was exposed in the headspace of a vial to allow adsorption of the drugs before gas chromatography. Recoveries of meperidine were 3 % for whole blood and 18 % for urine. Calibration curve for whole blood samples was linear in the range of 0.125-1μg/ml. The equation and ｒ value 0for the curve were: y=0.375 x + 0.0378 and r=0.993. The detection limit was about 0.1 and 0.02μg/ml for whole blood and urine, respectively.","subitem_description_language":"en","subitem_description_type":"Abstract"}]},"item_3_publisher_6":{"attribute_name":"出版者","attribute_value_mlt":[{"subitem_publisher":"日本法中毒学会","subitem_publisher_language":"ja"}]},"item_3_rights_7":{"attribute_name":"権利","attribute_value_mlt":[{"subitem_rights":"Copyright 日本法中毒学会","subitem_rights_language":"ja"},{"subitem_rights":"本文データは日本法中毒学会の許諾のもと掲載しています。","subitem_rights_language":"ja"}]},"item_3_source_id_19":{"attribute_name":"ISSN","attribute_value_mlt":[{"subitem_source_identifier":"09159606","subitem_source_identifier_type":"ISSN"}]},"item_3_version_type_32":{"attribute_name":"著者版フラグ","attribute_value_mlt":[{"subitem_version_resource":"http://purl.org/coar/version/c_970fb48d4fbd8a85","subitem_version_type":"VoR"}]},"item_creator":{"attribute_name":"著者","attribute_type":"creator","attribute_value_mlt":[{"creatorNames":[{"creatorName":"Seno, Hiroshi"}],"nameIdentifiers":[{"nameIdentifier":"3765","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"Kumazawa, Takeshi"}],"nameIdentifiers":[{"nameIdentifier":"3766","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"Ishii, Akira"}],"nameIdentifiers":[{"nameIdentifier":"3767","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"Nishikawa, Masanobu"}],"nameIdentifiers":[{"nameIdentifier":"3768","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"Hattori, Hideki"}],"nameIdentifiers":[{"nameIdentifier":"3769","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"Suzuki, Osamu"}],"nameIdentifiers":[{"nameIdentifier":"3770","nameIdentifierScheme":"WEKO"}]}]},"item_files":{"attribute_name":"ファイル情報","attribute_type":"file","attribute_value_mlt":[{"accessrole":"open_date","date":[{"dateType":"Available","dateValue":"2018-08-27"}],"displaytype":"detail","filename":"FT-13-211.pdf","filesize":[{"value":"191.2 kB"}],"format":"application/pdf","licensetype":"license_note","mimetype":"application/pdf","url":{"label":"FT-13-211.pdf","url":"https://hama-med.repo.nii.ac.jp/record/1668/files/FT-13-211.pdf"},"version_id":"33d77990-ff0d-4d84-a04f-74399bd18e99"}]},"item_keyword":{"attribute_name":"キーワード","attribute_value_mlt":[{"subitem_subject":"Solid phase microextraction (SPME)","subitem_subject_language":"en","subitem_subject_scheme":"Other"},{"subitem_subject":"Headspace method","subitem_subject_scheme":"Other"},{"subitem_subject":"Gas chromatography","subitem_subject_scheme":"Other"},{"subitem_subject":"Meperidine","subitem_subject_scheme":"Other"},{"subitem_subject":"Pethidine","subitem_subject_scheme":"Other"},{"subitem_subject":"Diphenylpyraline","subitem_subject_scheme":"Other"}]},"item_language":{"attribute_name":"言語","attribute_value_mlt":[{"subitem_language":"eng"}]},"item_resource_type":{"attribute_name":"資源タイプ","attribute_value_mlt":[{"resourcetype":"journal article","resourceuri":"http://purl.org/coar/resource_type/c_6501"}]},"item_title":"DETECTION OF MEPERIDINE (PETHIDINE) IN HUMAN BLOOD AND URINE BY HEADSPACE SOLID PHASE MICROEXTRACTION AND GAS CHROMATOGRAPHY","item_titles":{"attribute_name":"タイトル","attribute_value_mlt":[{"subitem_title":"DETECTION OF MEPERIDINE (PETHIDINE) IN HUMAN BLOOD AND URINE BY HEADSPACE SOLID PHASE MICROEXTRACTION AND GAS CHROMATOGRAPHY","subitem_title_language":"en"}]},"item_type_id":"3","owner":"4","path":["11"],"pubdate":{"attribute_name":"PubDate","attribute_value":"2013-08-27"},"publish_date":"2013-08-27","publish_status":"0","recid":"1668","relation_version_is_last":true,"title":["DETECTION OF MEPERIDINE (PETHIDINE) IN HUMAN BLOOD AND URINE BY HEADSPACE SOLID PHASE MICROEXTRACTION AND GAS CHROMATOGRAPHY"],"weko_creator_id":"4","weko_shared_id":-1},"updated":"2023-08-02T03:59:14.899495+00:00"}