{"created":"2023-06-20T15:47:08.261273+00:00","id":1678,"links":{},"metadata":{"_buckets":{"deposit":"1be5b2eb-0e0a-4994-8df3-8ca6f914c1cc"},"_deposit":{"created_by":4,"id":"1678","owners":[4],"pid":{"revision_id":0,"type":"depid","value":"1678"},"status":"published"},"_oai":{"id":"oai:hama-med.repo.nii.ac.jp:00001678","sets":["1:11"]},"author_link":["3824","3825","3826","3827","3828","3829"],"item_3_alternative_title_1":{"attribute_name":"その他のタイトル","attribute_value_mlt":[{"subitem_alternative_title":"Sensitive determination of thinner components in human body fluids by capillary gas chromatography with low oven temperature","subitem_alternative_title_language":"en"}]},"item_3_biblio_info_5":{"attribute_name":"書誌情報","attribute_value_mlt":[{"bibliographicIssueDates":{"bibliographicIssueDate":"1997-05-01","bibliographicIssueDateType":"Issued"},"bibliographicIssueNumber":"2","bibliographicPageEnd":"127","bibliographicPageStart":"126","bibliographicVolumeNumber":"15","bibliographic_titles":[{"bibliographic_title":"法中毒","bibliographic_titleLang":"ja"},{"bibliographic_title":"Japanese journal of forensic toxicology","bibliographic_titleLang":"en"}]}]},"item_3_description_9":{"attribute_name":"抄録","attribute_value_mlt":[{"subitem_description":"A sensitive method is presented for determination of thinner components in human body fluids by capillary gas chromatography (GC) with low oven temperature for trapping headspace vapor inside the capillary column. After heating a whole blood or urine sample containing ethyl acetate, benzene, n-butanol, toluene, n-butyl acetate n-isoamyl acetate and ethyl benzene as internal standard in a 7.5 ml-vial at 90 ℃ for 30 min, 5 ml of headspace vapor was drawn into a glass syringe. All vapor was introduced through an injection port in the splitless mode into a DB-624 middle-bore capillary column with the oven temperature at 5 ℃ for trapping all volatile compounds, and the oven temperature was programmed up to 110 ℃ for detection of the compounds by GC with a flame ionization detector. The present conditions gave sharp peaks and good separation of each compound with low background noises. Recoveries of the 6 compounds were 4.76-75.7% and 3.56-81.7% for whole blood and urine samples, respectively. The CV values of all compounds in whole blood and urine samples were 3.5-9.5 %. The calibration curves showed linearity in the range 0.78-400 ng/0.5 ml whole blood or urine; the detection limits were 0.5-5 ng/0.5 ml. The data on actual analysis of toluene and n-butyl acetate in postmortem blood were also presented.","subitem_description_language":"en","subitem_description_type":"Abstract"}]},"item_3_publisher_6":{"attribute_name":"出版者","attribute_value_mlt":[{"subitem_publisher":"日本法中毒学会","subitem_publisher_language":"ja"}]},"item_3_rights_7":{"attribute_name":"権利","attribute_value_mlt":[{"subitem_rights":"Copyright 日本法中毒学会","subitem_rights_language":"ja"},{"subitem_rights":"本文データは日本法中毒学会の許諾のもと掲載しています。","subitem_rights_language":"ja"}]},"item_3_source_id_19":{"attribute_name":"ISSN","attribute_value_mlt":[{"subitem_source_identifier":"09159606","subitem_source_identifier_type":"ISSN"}]},"item_3_version_type_32":{"attribute_name":"著者版フラグ","attribute_value_mlt":[{"subitem_version_resource":"http://purl.org/coar/version/c_970fb48d4fbd8a85","subitem_version_type":"VoR"}]},"item_creator":{"attribute_name":"著者","attribute_type":"creator","attribute_value_mlt":[{"creatorNames":[{"creatorName":"李, 暁鵬"}],"nameIdentifiers":[{}]},{"creatorNames":[{"creatorName":"熊澤, 武志"}],"nameIdentifiers":[{}]},{"creatorNames":[{"creatorName":"佐藤, 啓造"}],"nameIdentifiers":[{}]},{"creatorNames":[{"creatorName":"渡部, 加奈子"}],"nameIdentifiers":[{}]},{"creatorNames":[{"creatorName":"妹尾, 洋"}],"nameIdentifiers":[{}]},{"creatorNames":[{"creatorName":"鈴木, 修"}],"nameIdentifiers":[{}]}]},"item_files":{"attribute_name":"ファイル情報","attribute_type":"file","attribute_value_mlt":[{"accessrole":"open_date","date":[{"dateType":"Available","dateValue":"2018-08-27"}],"displaytype":"detail","filename":"FT-15-126.pdf","filesize":[{"value":"130.8 kB"}],"format":"application/pdf","licensetype":"license_note","mimetype":"application/pdf","url":{"label":"FT-15-126.pdf","url":"https://hama-med.repo.nii.ac.jp/record/1678/files/FT-15-126.pdf"},"version_id":"ca39f6a3-ba34-4093-ab7d-ad7358ccb769"}]},"item_language":{"attribute_name":"言語","attribute_value_mlt":[{"subitem_language":"jpn"}]},"item_resource_type":{"attribute_name":"資源タイプ","attribute_value_mlt":[{"resourcetype":"journal article","resourceuri":"http://purl.org/coar/resource_type/c_6501"}]},"item_title":"低温キャピラリーガスクロマトグラフィーによるシンナー成分の高感度分析","item_titles":{"attribute_name":"タイトル","attribute_value_mlt":[{"subitem_title":"低温キャピラリーガスクロマトグラフィーによるシンナー成分の高感度分析","subitem_title_language":"ja"}]},"item_type_id":"3","owner":"4","path":["11"],"pubdate":{"attribute_name":"PubDate","attribute_value":"2013-08-27"},"publish_date":"2013-08-27","publish_status":"0","recid":"1678","relation_version_is_last":true,"title":["低温キャピラリーガスクロマトグラフィーによるシンナー成分の高感度分析"],"weko_creator_id":"4","weko_shared_id":-1},"updated":"2023-08-02T03:59:38.659369+00:00"}