@article{oai:hama-med.repo.nii.ac.jp:00001679,
 author = {渡部, 加奈子 and 石井, 晃 and 妹尾, 洋 and 鈴木, 修 and 服部, 秀樹},
 issue = {2},
 journal = {法中毒, Japanese journal of forensic toxicology},
 month = {May},
 note = {A new method of gas chromatography(GC), for measurments of chloroform or methylene chloride in whole blood which allowed us to introduce as much as a 5 ml volume of headspace vapor without any loss, is presented with use of a low oven temperature (- 30℃). After heating a blood sample containing the two drugs (internal standard, vice versa) in a 7.0 ml vial at 55℃ for 20 min, 5 ml of the headspace vapor was drawn into a glass syringe. All vapor was introduced through an injection port in the splittless mode into an RtxVolatiles middle-bore capillary column at -30℃ of oven temperature for trapping entire amounts of compounds to be analyzed and the oven temperature was programmed up to 280℃ for detection of the compounds. The present conditions gave sharp peaks for both compounds and very low background noises for whole blood samples. The calibration curves showed linearity in the range of 0.01- 5.0 ug/ 0.5 ml whole blood. The detection limit was about 2 ng /0.5 ug whole blood.},
 pages = {128--129},
 title = {低温キャピラリーガスクロマトグラフィーによるクロロホルム、メチレンクロライドの高感度分析},
 volume = {15},
 year = {1997}
}