{"created":"2023-06-20T15:47:08.332728+00:00","id":1679,"links":{},"metadata":{"_buckets":{"deposit":"4d90524d-c8a5-4ab1-be73-cf7a4d8a5ffe"},"_deposit":{"created_by":4,"id":"1679","owners":[4],"pid":{"revision_id":0,"type":"depid","value":"1679"},"status":"published"},"_oai":{"id":"oai:hama-med.repo.nii.ac.jp:00001679","sets":["1:11"]},"author_link":["3830","3831","3832","3833","3834"],"item_3_alternative_title_1":{"attribute_name":"その他のタイトル","attribute_value_mlt":[{"subitem_alternative_title":"SENSITIVE DETERMINATION OF CHLOROFORM AND METHYLENE CHLORIDE IN WHOLE BLOOD BY CAPILLARY GAS CHROMATOGRAPHY WITH CRYOGENIC OVEN TEMPERATURE","subitem_alternative_title_language":"en"}]},"item_3_biblio_info_5":{"attribute_name":"書誌情報","attribute_value_mlt":[{"bibliographicIssueDates":{"bibliographicIssueDate":"1997-05-01","bibliographicIssueDateType":"Issued"},"bibliographicIssueNumber":"2","bibliographicPageEnd":"129","bibliographicPageStart":"128","bibliographicVolumeNumber":"15","bibliographic_titles":[{"bibliographic_title":"法中毒","bibliographic_titleLang":"ja"},{"bibliographic_title":"Japanese journal of forensic toxicology","bibliographic_titleLang":"en"}]}]},"item_3_description_9":{"attribute_name":"抄録","attribute_value_mlt":[{"subitem_description":"A new method of gas chromatography(GC), for measurments of chloroform or methylene chloride in whole blood which allowed us to introduce as much as a 5 ml volume of headspace vapor without any loss, is presented with use of a low oven temperature (- 30℃). After heating a blood sample containing the two drugs (internal standard, vice versa) in a 7.0 ml vial at 55℃ for 20 min, 5 ml of the headspace vapor was drawn into a glass syringe. All vapor was introduced through an injection port in the splittless mode into an RtxVolatiles middle-bore capillary column at -30℃ of oven temperature for trapping entire amounts of compounds to be analyzed and the oven temperature was programmed up to 280℃ for detection of the compounds. The present conditions gave sharp peaks for both compounds and very low background noises for whole blood samples. The calibration curves showed linearity in the range of 0.01- 5.0 ug/ 0.5 ml whole blood. The detection limit was about 2 ng /0.5 ug whole blood.","subitem_description_language":"en","subitem_description_type":"Abstract"}]},"item_3_publisher_6":{"attribute_name":"出版者","attribute_value_mlt":[{"subitem_publisher":"日本法中毒学会","subitem_publisher_language":"ja"}]},"item_3_rights_7":{"attribute_name":"権利","attribute_value_mlt":[{"subitem_rights":"Copyright 日本法中毒学会","subitem_rights_language":"ja"},{"subitem_rights":"本文データは日本法中毒学会の許諾のもと掲載しています。","subitem_rights_language":"ja"}]},"item_3_source_id_19":{"attribute_name":"ISSN","attribute_value_mlt":[{"subitem_source_identifier":"09159606","subitem_source_identifier_type":"ISSN"}]},"item_3_version_type_32":{"attribute_name":"著者版フラグ","attribute_value_mlt":[{"subitem_version_resource":"http://purl.org/coar/version/c_970fb48d4fbd8a85","subitem_version_type":"VoR"}]},"item_creator":{"attribute_name":"著者","attribute_type":"creator","attribute_value_mlt":[{"creatorNames":[{"creatorName":"渡部, 加奈子"}],"nameIdentifiers":[{"nameIdentifier":"3830","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"石井, 晃"}],"nameIdentifiers":[{"nameIdentifier":"3831","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"妹尾, 洋"}],"nameIdentifiers":[{"nameIdentifier":"3832","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"鈴木, 修"}],"nameIdentifiers":[{"nameIdentifier":"3833","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"服部, 秀樹"}],"nameIdentifiers":[{"nameIdentifier":"3834","nameIdentifierScheme":"WEKO"}]}]},"item_files":{"attribute_name":"ファイル情報","attribute_type":"file","attribute_value_mlt":[{"accessrole":"open_date","date":[{"dateType":"Available","dateValue":"2018-08-27"}],"displaytype":"detail","filename":"FT-15-128.pdf","filesize":[{"value":"102.4 kB"}],"format":"application/pdf","licensetype":"license_note","mimetype":"application/pdf","url":{"label":"FT-15-128.pdf","url":"https://hama-med.repo.nii.ac.jp/record/1679/files/FT-15-128.pdf"},"version_id":"c4e4e971-d4be-4cfe-805d-b41391b0ffdc"}]},"item_language":{"attribute_name":"言語","attribute_value_mlt":[{"subitem_language":"jpn"}]},"item_resource_type":{"attribute_name":"資源タイプ","attribute_value_mlt":[{"resourcetype":"journal article","resourceuri":"http://purl.org/coar/resource_type/c_6501"}]},"item_title":"低温キャピラリーガスクロマトグラフィーによるクロロホルム、メチレンクロライドの高感度分析","item_titles":{"attribute_name":"タイトル","attribute_value_mlt":[{"subitem_title":"低温キャピラリーガスクロマトグラフィーによるクロロホルム、メチレンクロライドの高感度分析","subitem_title_language":"ja"}]},"item_type_id":"3","owner":"4","path":["11"],"pubdate":{"attribute_name":"PubDate","attribute_value":"2013-08-27"},"publish_date":"2013-08-27","publish_status":"0","recid":"1679","relation_version_is_last":true,"title":["低温キャピラリーガスクロマトグラフィーによるクロロホルム、メチレンクロライドの高感度分析"],"weko_creator_id":"4","weko_shared_id":-1},"updated":"2023-08-02T03:59:39.679666+00:00"}