{"created":"2023-06-20T15:47:08.474542+00:00","id":1681,"links":{},"metadata":{"_buckets":{"deposit":"24d05910-9fce-4221-80a3-31e8c35a6927"},"_deposit":{"created_by":4,"id":"1681","owners":[4],"pid":{"revision_id":0,"type":"depid","value":"1681"},"status":"published"},"_oai":{"id":"oai:hama-med.repo.nii.ac.jp:00001681","sets":["1:11"]},"author_link":["3842","3843","3844","3845","3846","3847"],"item_3_alternative_title_1":{"attribute_name":"その他のタイトル","attribute_value_mlt":[{"subitem_alternative_title":"低温トラッピングキャピラリーガスクロマトグラフィーによる血中尿中トリクロロエチレンの高感度定量","subitem_alternative_title_language":"ja"}]},"item_3_biblio_info_5":{"attribute_name":"書誌情報","attribute_value_mlt":[{"bibliographicIssueDates":{"bibliographicIssueDate":"1997-09-16","bibliographicIssueDateType":"Issued"},"bibliographicIssueNumber":"3","bibliographicPageEnd":"216","bibliographicPageStart":"211","bibliographicVolumeNumber":"15","bibliographic_titles":[{"bibliographic_title":"法中毒","bibliographic_titleLang":"ja"},{"bibliographic_title":"Japanese journal of forensic toxicology","bibliographic_titleLang":"en"}]}]},"item_3_description_9":{"attribute_name":"抄録","attribute_value_mlt":[{"subitem_description":"A new and sensitive method for measurements of trichloroethylene in blood and urine by capillary gas chromatography (GC) with cryogenic trapping is presented. After heating a body fluid samples (1ml) containing trichloroethylene and tetrachloroethylene (internal standard. IS) in a 7.0-ml vial at 55℃ for 20 min, 5 ml of the headspace vapor was drawn into a glass syringe. All vapor was introduced into an Rtx-Volatiles middle-bore capillary column in the splitless mode at 0 ℃ of oven temperature to trap the entire analytes. and the oven temperature was programmed up to 270℃. The present conditions gave sharp peaks for both trichloroethylene and tetrachloroethylene (IS), and low background noises for whole blood and urine samples. As much as 75.0 and 63.1 % of trichloroethylene and IS. respectively, which had been added to whole blood in a vial, could be introduced into the GC column. The calibration curves showed linearity in the range of 0.5-5.0μg/ml for both whole blood and urine. The detection limit was as low as about 3 ng/ml of whole blood.","subitem_description_language":"en","subitem_description_type":"Abstract"}]},"item_3_publisher_6":{"attribute_name":"出版者","attribute_value_mlt":[{"subitem_publisher":"日本法中毒学会","subitem_publisher_language":"ja"}]},"item_3_rights_7":{"attribute_name":"権利","attribute_value_mlt":[{"subitem_rights":"Copyright 日本法中毒学会","subitem_rights_language":"ja"},{"subitem_rights":"本文データは日本法中毒学会の許諾のもと掲載しています。","subitem_rights_language":"ja"}]},"item_3_source_id_19":{"attribute_name":"ISSN","attribute_value_mlt":[{"subitem_source_identifier":"09159606","subitem_source_identifier_type":"ISSN"}]},"item_3_version_type_32":{"attribute_name":"著者版フラグ","attribute_value_mlt":[{"subitem_version_resource":"http://purl.org/coar/version/c_970fb48d4fbd8a85","subitem_version_type":"VoR"}]},"item_creator":{"attribute_name":"著者","attribute_type":"creator","attribute_value_mlt":[{"creatorNames":[{"creatorName":"Watanabe, Kanako"}],"nameIdentifiers":[{"nameIdentifier":"3842","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"Seno, Hiroshi"}],"nameIdentifiers":[{"nameIdentifier":"3843","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"Ishii, Akira"}],"nameIdentifiers":[{"nameIdentifier":"3844","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"Kumazawa, Takeshi"}],"nameIdentifiers":[{"nameIdentifier":"3845","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"Hattori, Hideki"}],"nameIdentifiers":[{"nameIdentifier":"3846","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"Suzuki, Osamu"}],"nameIdentifiers":[{"nameIdentifier":"3847","nameIdentifierScheme":"WEKO"}]}]},"item_files":{"attribute_name":"ファイル情報","attribute_type":"file","attribute_value_mlt":[{"accessrole":"open_date","date":[{"dateType":"Available","dateValue":"2018-08-27"}],"displaytype":"detail","filename":"FT-15-211.pdf","filesize":[{"value":"235.0 kB"}],"format":"application/pdf","licensetype":"license_note","mimetype":"application/pdf","url":{"label":"FT-15-211.pdf","url":"https://hama-med.repo.nii.ac.jp/record/1681/files/FT-15-211.pdf"},"version_id":"999bf0ed-c373-4abc-a37d-7f3fe8f3b7eb"}]},"item_keyword":{"attribute_name":"キーワード","attribute_value_mlt":[{"subitem_subject":"Trichloroethylene","subitem_subject_language":"en","subitem_subject_scheme":"Other"},{"subitem_subject":"Tetrachloroethylene","subitem_subject_scheme":"Other"},{"subitem_subject":"Gas chromatography","subitem_subject_scheme":"Other"},{"subitem_subject":"Cryogenic trapping","subitem_subject_scheme":"Other"},{"subitem_subject":"Headspace method","subitem_subject_scheme":"Other"}]},"item_language":{"attribute_name":"言語","attribute_value_mlt":[{"subitem_language":"eng"}]},"item_resource_type":{"attribute_name":"資源タイプ","attribute_value_mlt":[{"resourcetype":"journal article","resourceuri":"http://purl.org/coar/resource_type/c_6501"}]},"item_title":"SENSITIVE DETERMINATION OF TRICHLOROETHYLENE IN BLOOD AND URINE BY CAPILLARY GAS CHROMATOGRAPHY WITH CRYOGENIC TRAPPING","item_titles":{"attribute_name":"タイトル","attribute_value_mlt":[{"subitem_title":"SENSITIVE DETERMINATION OF TRICHLOROETHYLENE IN BLOOD AND URINE BY CAPILLARY GAS CHROMATOGRAPHY WITH CRYOGENIC TRAPPING","subitem_title_language":"en"}]},"item_type_id":"3","owner":"4","path":["11"],"pubdate":{"attribute_name":"PubDate","attribute_value":"2013-08-27"},"publish_date":"2013-08-27","publish_status":"0","recid":"1681","relation_version_is_last":true,"title":["SENSITIVE DETERMINATION OF TRICHLOROETHYLENE IN BLOOD AND URINE BY CAPILLARY GAS CHROMATOGRAPHY WITH CRYOGENIC TRAPPING"],"weko_creator_id":"4","weko_shared_id":-1},"updated":"2023-08-02T03:59:44.521845+00:00"}