{"created":"2023-06-20T15:47:08.615776+00:00","id":1683,"links":{},"metadata":{"_buckets":{"deposit":"ef1cf5cf-ea1c-420a-946a-c267d43df358"},"_deposit":{"created_by":4,"id":"1683","owners":[4],"pid":{"revision_id":0,"type":"depid","value":"1683"},"status":"published"},"_oai":{"id":"oai:hama-med.repo.nii.ac.jp:00001683","sets":["1:11"]},"author_link":["3853","3854","3855","3856","3857","3858"],"item_3_alternative_title_1":{"attribute_name":"その他のタイトル","attribute_value_mlt":[{"subitem_alternative_title":"低温トラッピングキャピラリーガスクロマトグラフィーによる血中エチルエーテルの高感度定量","subitem_alternative_title_language":"ja"}]},"item_3_biblio_info_5":{"attribute_name":"書誌情報","attribute_value_mlt":[{"bibliographicIssueDates":{"bibliographicIssueDate":"1998-01-31","bibliographicIssueDateType":"Issued"},"bibliographicIssueNumber":"1","bibliographicPageEnd":"74","bibliographicPageStart":"69","bibliographicVolumeNumber":"16","bibliographic_titles":[{"bibliographic_title":"法中毒","bibliographic_titleLang":"ja"},{"bibliographic_title":"Japanese journal of forensic toxicology","bibliographic_titleLang":"en"}]}]},"item_3_description_9":{"attribute_name":"抄録","attribute_value_mlt":[{"subitem_description":"A new and sensitive method for measurements of ethyl ether in whole blood by capillary gas chromatography (GC) with cryogenic trapping is presented. After heating a body fluid sample (1ml) containing ethyl ether and propyl ether (internal standard, IS) in a 7.0-ml vial at 55℃ for 20 min, 5 ml of the headspace vapor was drawn into a glass syringe. All vapor was introduced into an Rtx-Volatiles middle-bore capillary column in the splitless mode at -50℃ of oven temperature to trap the entire analytes, and the oven temperature was programmed up to 260℃. The present conditions gave sharp peaks for both ethyl ether and propyl ether (IS) , and low background noises for whole blood samples. As much as 53.9 and 38.3 % of ethyl ether and IS, respectively, which had been added to whole blood in a vial, could be introduced into the GC column. The calibration curves showed linearity in the range of 0.5-5.0μg / ml whole blood. The detection limit was as low as about 10 ng/ml whole blood.","subitem_description_language":"en","subitem_description_type":"Abstract"}]},"item_3_publisher_6":{"attribute_name":"出版者","attribute_value_mlt":[{"subitem_publisher":"日本法中毒学会","subitem_publisher_language":"ja"}]},"item_3_rights_7":{"attribute_name":"権利","attribute_value_mlt":[{"subitem_rights":"Copyright 日本法中毒学会","subitem_rights_language":"ja"},{"subitem_rights":"本文データは日本法中毒学会の許諾のもと掲載しています。","subitem_rights_language":"ja"}]},"item_3_source_id_19":{"attribute_name":"ISSN","attribute_value_mlt":[{"subitem_source_identifier":"09159606","subitem_source_identifier_type":"ISSN"}]},"item_3_version_type_32":{"attribute_name":"著者版フラグ","attribute_value_mlt":[{"subitem_version_resource":"http://purl.org/coar/version/c_970fb48d4fbd8a85","subitem_version_type":"VoR"}]},"item_creator":{"attribute_name":"著者","attribute_type":"creator","attribute_value_mlt":[{"creatorNames":[{"creatorName":"Watanabe, Kanako"}],"nameIdentifiers":[{"nameIdentifier":"3853","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"Seno, Hiroshi"}],"nameIdentifiers":[{"nameIdentifier":"3854","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"Ishii, Akira"}],"nameIdentifiers":[{"nameIdentifier":"3855","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"Kumazawa, Takeshi"}],"nameIdentifiers":[{"nameIdentifier":"3856","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"Hattori, Hideki"}],"nameIdentifiers":[{"nameIdentifier":"3857","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"Suzuki, Osamu"}],"nameIdentifiers":[{"nameIdentifier":"3858","nameIdentifierScheme":"WEKO"}]}]},"item_files":{"attribute_name":"ファイル情報","attribute_type":"file","attribute_value_mlt":[{"accessrole":"open_date","date":[{"dateType":"Available","dateValue":"2018-08-27"}],"displaytype":"detail","filename":"FT-16-69.pdf","filesize":[{"value":"218.2 kB"}],"format":"application/pdf","licensetype":"license_note","mimetype":"application/pdf","url":{"label":"FT-16-69.pdf","url":"https://hama-med.repo.nii.ac.jp/record/1683/files/FT-16-69.pdf"},"version_id":"fcc21a2f-00e1-4a69-8e74-5097a35f0aa8"}]},"item_keyword":{"attribute_name":"キーワード","attribute_value_mlt":[{"subitem_subject":"Ethyl ether","subitem_subject_language":"en","subitem_subject_scheme":"Other"},{"subitem_subject":"Propyl ether","subitem_subject_scheme":"Other"},{"subitem_subject":"Gas chromatography","subitem_subject_scheme":"Other"},{"subitem_subject":"Cryogenic trapping","subitem_subject_scheme":"Other"},{"subitem_subject":"Headspace method","subitem_subject_scheme":"Other"}]},"item_language":{"attribute_name":"言語","attribute_value_mlt":[{"subitem_language":"eng"}]},"item_resource_type":{"attribute_name":"資源タイプ","attribute_value_mlt":[{"resourcetype":"journal article","resourceuri":"http://purl.org/coar/resource_type/c_6501"}]},"item_title":"SENSITIVE DETERMINATION OF ETHYL ETHER IN WHOLE BLOOD BY CAPILLARY GAS CHROMATOGRAPHY WITH CRYOGENIC TRAPPING","item_titles":{"attribute_name":"タイトル","attribute_value_mlt":[{"subitem_title":"SENSITIVE DETERMINATION OF ETHYL ETHER IN WHOLE BLOOD BY CAPILLARY GAS CHROMATOGRAPHY WITH CRYOGENIC TRAPPING","subitem_title_language":"en"}]},"item_type_id":"3","owner":"4","path":["11"],"pubdate":{"attribute_name":"PubDate","attribute_value":"2013-08-27"},"publish_date":"2013-08-27","publish_status":"0","recid":"1683","relation_version_is_last":true,"title":["SENSITIVE DETERMINATION OF ETHYL ETHER IN WHOLE BLOOD BY CAPILLARY GAS CHROMATOGRAPHY WITH CRYOGENIC TRAPPING"],"weko_creator_id":"4","weko_shared_id":-1},"updated":"2023-08-02T03:59:49.326073+00:00"}