{"created":"2023-06-20T15:47:09.074417+00:00","id":1692,"links":{},"metadata":{"_buckets":{"deposit":"117dc639-0948-4250-b8df-190f5d3da657"},"_deposit":{"created_by":4,"id":"1692","owners":[4],"pid":{"revision_id":0,"type":"depid","value":"1692"},"status":"published"},"_oai":{"id":"oai:hama-med.repo.nii.ac.jp:00001692","sets":["1:11"]},"author_link":["3904","3905","3906","3907","3908"],"item_3_alternative_title_1":{"attribute_name":"その他のタイトル","attribute_value_mlt":[{"subitem_alternative_title":"DETERMINATION OF CRESOL ISOMERS AND PHENOL BY CAPILLARY GAS CHROMATOGRAPHY WITH CRYOGENIC OVEN TRAPPING","subitem_alternative_title_language":"en"}]},"item_3_biblio_info_5":{"attribute_name":"書誌情報","attribute_value_mlt":[{"bibliographicIssueDates":{"bibliographicIssueDate":"2000-05-15","bibliographicIssueDateType":"Issued"},"bibliographicIssueNumber":"2","bibliographicPageEnd":"137","bibliographicPageStart":"136","bibliographicVolumeNumber":"18","bibliographic_titles":[{"bibliographic_title":"法中毒","bibliographic_titleLang":"ja"},{"bibliographic_title":"Japanese journal of forensic toxicology","bibliographic_titleLang":"en"}]}]},"item_3_description_9":{"attribute_name":"抄録","attribute_value_mlt":[{"subitem_description":"A simple method for determination of o-cresol, m-cresol, p-cresol and phenol from human body fluids by capillary gas chromatography (GC) has been developed using cryogenic oven trapping. After heating a whole blood or urine sample containing the four compounds and 2,4-dimethylphenol as internal standard in a 7.5 ml-vial at 100℃ for 10 min, 5 ml of headspace vapor was drawn into a gas tight syringe. All vapor was introduced through an injection port of a GC instrument in the splitless mode into an α-DEX 120 middle-bore capillary column at 0℃ of oven temperature for trapping the compounds; the oven temperature was programmed up to 170℃ for their detection by GC with flame ionization detection. The present conditions gave sharp peaks for the compounds, a good separation of each peak and low background impurities for whole blood and urine samples. The extraction efficiencies of the compounds were 0.25-0.68 % for whole blood and 0.51-1.14 % for urine. The calibration curves for all compounds showed good linearity in the range 1-10 μg/0.5 mｌ and the detection limits were 0.3-0.5μg/0.5 mｌ.","subitem_description_language":"en","subitem_description_type":"Abstract"}]},"item_3_publisher_6":{"attribute_name":"出版者","attribute_value_mlt":[{"subitem_publisher":"日本法中毒学会","subitem_publisher_language":"ja"}]},"item_3_rights_7":{"attribute_name":"権利","attribute_value_mlt":[{"subitem_rights":"Copyright 日本法中毒学会","subitem_rights_language":"ja"},{"subitem_rights":"本文データは日本法中毒学会の許諾のもと掲載しています。","subitem_rights_language":"ja"}]},"item_3_source_id_19":{"attribute_name":"ISSN","attribute_value_mlt":[{"subitem_source_identifier":"09159606","subitem_source_identifier_type":"ISSN"}]},"item_3_version_type_32":{"attribute_name":"著者版フラグ","attribute_value_mlt":[{"subitem_version_resource":"http://purl.org/coar/version/c_970fb48d4fbd8a85","subitem_version_type":"VoR"}]},"item_creator":{"attribute_name":"著者","attribute_type":"creator","attribute_value_mlt":[{"creatorNames":[{"creatorName":"李, 暁鵬"}],"nameIdentifiers":[{}]},{"creatorNames":[{"creatorName":"熊澤, 武志"}],"nameIdentifiers":[{}]},{"creatorNames":[{"creatorName":"近藤, 圭"}],"nameIdentifiers":[{}]},{"creatorNames":[{"creatorName":"佐藤, 啓造"}],"nameIdentifiers":[{}]},{"creatorNames":[{"creatorName":"鈴木, 修"}],"nameIdentifiers":[{}]}]},"item_files":{"attribute_name":"ファイル情報","attribute_type":"file","attribute_value_mlt":[{"accessrole":"open_date","date":[{"dateType":"Available","dateValue":"2018-08-27"}],"displaytype":"detail","filename":"FT-18-136.pdf","filesize":[{"value":"131.5 kB"}],"format":"application/pdf","licensetype":"license_note","mimetype":"application/pdf","url":{"label":"FT-18-136.pdf","url":"https://hama-med.repo.nii.ac.jp/record/1692/files/FT-18-136.pdf"},"version_id":"7d284d6d-01f1-406b-a975-c3dcaf1223c4"}]},"item_language":{"attribute_name":"言語","attribute_value_mlt":[{"subitem_language":"jpn"}]},"item_resource_type":{"attribute_name":"資源タイプ","attribute_value_mlt":[{"resourcetype":"journal article","resourceuri":"http://purl.org/coar/resource_type/c_6501"}]},"item_title":"低温オーブントラッピングキャピラリーガスクロマトグラフィーによるクレゾール異性体およびフェノールの分析","item_titles":{"attribute_name":"タイトル","attribute_value_mlt":[{"subitem_title":"低温オーブントラッピングキャピラリーガスクロマトグラフィーによるクレゾール異性体およびフェノールの分析","subitem_title_language":"ja"}]},"item_type_id":"3","owner":"4","path":["11"],"pubdate":{"attribute_name":"PubDate","attribute_value":"2013-08-27"},"publish_date":"2013-08-27","publish_status":"0","recid":"1692","relation_version_is_last":true,"title":["低温オーブントラッピングキャピラリーガスクロマトグラフィーによるクレゾール異性体およびフェノールの分析"],"weko_creator_id":"4","weko_shared_id":-1},"updated":"2023-08-02T04:00:13.652858+00:00"}