{"created":"2023-06-20T15:47:09.353391+00:00","id":1698,"links":{},"metadata":{"_buckets":{"deposit":"1a23457f-d394-4165-b45c-472726199d58"},"_deposit":{"created_by":4,"id":"1698","owners":[4],"pid":{"revision_id":0,"type":"depid","value":"1698"},"status":"published"},"_oai":{"id":"oai:hama-med.repo.nii.ac.jp:00001698","sets":["1:11"]},"author_link":["3942","3943","3944","3945","3946"],"item_3_alternative_title_1":{"attribute_name":"その他のタイトル","attribute_value_mlt":[{"subitem_alternative_title":"Sensitive determination of styrene and related compounds in human body fluids by headspace capillary gas chromatography with cryogenic oven trapping","subitem_alternative_title_language":"en"}]},"item_3_biblio_info_5":{"attribute_name":"書誌情報","attribute_value_mlt":[{"bibliographicIssueDates":{"bibliographicIssueDate":"2001-05-15","bibliographicIssueDateType":"Issued"},"bibliographicIssueNumber":"2","bibliographicPageEnd":"183","bibliographicPageStart":"182","bibliographicVolumeNumber":"19","bibliographic_titles":[{"bibliographic_title":"法中毒","bibliographic_titleLang":"ja"},{"bibliographic_title":"Japanese journal of forensic toxicology","bibliographic_titleLang":"en"}]}]},"item_3_description_9":{"attribute_name":"抄録","attribute_value_mlt":[{"subitem_description":"A simple and sensitive method is presented for determination of styrene, toluene, ethylbenzene, isopropylbenzene and n-propylbenzene in human body fluids by capillary gas chromatography (GC) with cryogenic oven trapping. After heating a blood or urine sample containing each compound and p-diethylbenzene (IS) in a 7.0-ml vial at 60℃ for 20 min, 5 ml of the headspace vapor was drawn into a glass syringe and injected into a GC port. All vapor was introduced into an Rtx-Volatile middle bore capillary column in the splitless mode at 20℃ of oven temperature to trap entire analytes, and then the oven temperature was programmed up to 280℃ for GC measurements by with flame ionization detection. The present conditions gave sharp peaks of each compound and IS, and low background noises for whole blood or urine samples. Each compound could be determined for rat whole blood after inhalation of gas of the five compounds. The present GC with cryogenic oven trapping is recommendable for use in determinations of styrene and related compounds in forensic and environmental toxicology, because it is simple, requires no special GC operations and gives high sensitivity and good separations.","subitem_description_language":"en","subitem_description_type":"Abstract"}]},"item_3_publisher_6":{"attribute_name":"出版者","attribute_value_mlt":[{"subitem_publisher":"日本法中毒学会","subitem_publisher_language":"ja"}]},"item_3_rights_7":{"attribute_name":"権利","attribute_value_mlt":[{"subitem_rights":"Copyright 日本法中毒学会","subitem_rights_language":"ja"},{"subitem_rights":"本文データは日本法中毒学会の許諾のもと掲載しています。","subitem_rights_language":"ja"}]},"item_3_source_id_19":{"attribute_name":"ISSN","attribute_value_mlt":[{"subitem_source_identifier":"09159606","subitem_source_identifier_type":"ISSN"}]},"item_3_version_type_32":{"attribute_name":"著者版フラグ","attribute_value_mlt":[{"subitem_version_resource":"http://purl.org/coar/version/c_970fb48d4fbd8a85","subitem_version_type":"VoR"}]},"item_creator":{"attribute_name":"著者","attribute_type":"creator","attribute_value_mlt":[{"creatorNames":[{"creatorName":"渡部, 加奈子"}],"nameIdentifiers":[{}]},{"creatorNames":[{"creatorName":"鈴木, 修"}],"nameIdentifiers":[{}]},{"creatorNames":[{"creatorName":"石井, 晃"}],"nameIdentifiers":[{}]},{"creatorNames":[{"creatorName":"妹尾, 洋"}],"nameIdentifiers":[{}]},{"creatorNames":[{"creatorName":"鈴木, 加奈子"}],"nameIdentifiers":[{}]}]},"item_files":{"attribute_name":"ファイル情報","attribute_type":"file","attribute_value_mlt":[{"accessrole":"open_date","date":[{"dateType":"Available","dateValue":"2018-08-27"}],"displaytype":"detail","filename":"FT-19-182.pdf","filesize":[{"value":"144.7 kB"}],"format":"application/pdf","licensetype":"license_note","mimetype":"application/pdf","url":{"label":"FT-19-182.pdf","url":"https://hama-med.repo.nii.ac.jp/record/1698/files/FT-19-182.pdf"},"version_id":"8db25104-46fa-41b5-a2bd-ca1ce457b29e"}]},"item_language":{"attribute_name":"言語","attribute_value_mlt":[{"subitem_language":"jpn"}]},"item_resource_type":{"attribute_name":"資源タイプ","attribute_value_mlt":[{"resourcetype":"journal article","resourceuri":"http://purl.org/coar/resource_type/c_6501"}]},"item_title":"低温オーブントラッピングガスクロマトグラフィーによるヒト体液中スチレン及び関連物質の高感度分析","item_titles":{"attribute_name":"タイトル","attribute_value_mlt":[{"subitem_title":"低温オーブントラッピングガスクロマトグラフィーによるヒト体液中スチレン及び関連物質の高感度分析","subitem_title_language":"ja"}]},"item_type_id":"3","owner":"4","path":["11"],"pubdate":{"attribute_name":"PubDate","attribute_value":"2013-08-27"},"publish_date":"2013-08-27","publish_status":"0","recid":"1698","relation_version_is_last":true,"title":["低温オーブントラッピングガスクロマトグラフィーによるヒト体液中スチレン及び関連物質の高感度分析"],"weko_creator_id":"4","weko_shared_id":-1},"updated":"2023-08-02T04:00:27.805830+00:00"}