{"created":"2023-06-20T15:47:09.971705+00:00","id":1707,"links":{},"metadata":{"_buckets":{"deposit":"e96f6c1d-8527-44f2-bfb7-163714180911"},"_deposit":{"created_by":4,"id":"1707","owners":[4],"pid":{"revision_id":0,"type":"depid","value":"1707"},"status":"published"},"_oai":{"id":"oai:hama-med.repo.nii.ac.jp:00001707","sets":["1:11"]},"author_link":["3998","3999","4000","4001","4002"],"item_3_alternative_title_1":{"attribute_name":"その他のタイトル","attribute_value_mlt":[{"subitem_alternative_title":"新内面逆相ODSカラムを用いた血清中モルヒネ，コデインならびにコカインのLS/MSによる定量","subitem_alternative_title_language":"ja"}]},"item_3_biblio_info_5":{"attribute_name":"書誌情報","attribute_value_mlt":[{"bibliographicIssueDates":{"bibliographicIssueDate":"2003-01-31","bibliographicIssueDateType":"Issued"},"bibliographicIssueNumber":"1","bibliographicPageEnd":"54","bibliographicPageStart":"47","bibliographicVolumeNumber":"21","bibliographic_titles":[{"bibliographic_title":"法中毒","bibliographic_titleLang":"ja"},{"bibliographic_title":"Japanese journal of forensic toxicology","bibliographic_titleLang":"en"}]}]},"item_3_description_9":{"attribute_name":"抄録","attribute_value_mlt":[{"subitem_description":"A new internal surface reversed phase column (Shim-pack MAYI-ODS) was used for analysis of morphine, codeine and cocaine in human sera by LC/MS/MS. The column enabled direct injection of crude biological samples without pretreatment realizing a rapid analytical procedure. The recoveries of morphine, codeine and cocaine spiked into human sera were 50-60 %. The regression equations for morphine, codeine and cocaine in sera, using atropine as internal standard, showed good linearity in the ranges of 100-500. 50-250 and 20-100 ng/ml, respectively; the detection limits were 50, 20 and 10 ng/ml, respectively. The coefficients of intra-day variation for the three compounds spiked into sera were less than 7 %. The proposed method seems useful for toxicological analysis of three drugs, because of rapidness and reproducibility.","subitem_description_language":"en","subitem_description_type":"Abstract"}]},"item_3_publisher_6":{"attribute_name":"出版者","attribute_value_mlt":[{"subitem_publisher":"日本法中毒学会","subitem_publisher_language":"ja"}]},"item_3_rights_7":{"attribute_name":"権利","attribute_value_mlt":[{"subitem_rights":"Copyright 日本法中毒学会","subitem_rights_language":"ja"},{"subitem_rights":"本文データは日本法中毒学会の許諾のもと掲載しています。","subitem_rights_language":"ja"}]},"item_3_source_id_19":{"attribute_name":"ISSN","attribute_value_mlt":[{"subitem_source_identifier":"09159606","subitem_source_identifier_type":"ISSN"}]},"item_3_version_type_32":{"attribute_name":"著者版フラグ","attribute_value_mlt":[{"subitem_version_resource":"http://purl.org/coar/version/c_970fb48d4fbd8a85","subitem_version_type":"VoR"}]},"item_creator":{"attribute_name":"著者","attribute_type":"creator","attribute_value_mlt":[{"creatorNames":[{"creatorName":"Hattori, Hideki"}],"nameIdentifiers":[{"nameIdentifier":"3998","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"Arinobu, Tetsuya"}],"nameIdentifiers":[{"nameIdentifier":"3999","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"Iwai, Masae"}],"nameIdentifiers":[{"nameIdentifier":"4000","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"Suzuki, Osamu"}],"nameIdentifiers":[{"nameIdentifier":"4001","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"Seno, Hiroshi"}],"nameIdentifiers":[{"nameIdentifier":"4002","nameIdentifierScheme":"WEKO"}]}]},"item_files":{"attribute_name":"ファイル情報","attribute_type":"file","attribute_value_mlt":[{"accessrole":"open_date","date":[{"dateType":"Available","dateValue":"2018-08-27"}],"displaytype":"detail","filename":"FT-21-47.pdf","filesize":[{"value":"277.1 kB"}],"format":"application/pdf","licensetype":"license_note","mimetype":"application/pdf","url":{"label":"FT-21-47.pdf","url":"https://hama-med.repo.nii.ac.jp/record/1707/files/FT-21-47.pdf"},"version_id":"d46e1a53-f165-4b8c-bee8-77e601d0ae6f"}]},"item_keyword":{"attribute_name":"キーワード","attribute_value_mlt":[{"subitem_subject":"Morphine","subitem_subject_scheme":"Other"},{"subitem_subject":"Codeine","subitem_subject_scheme":"Other"},{"subitem_subject":"Cocaine","subitem_subject_scheme":"Other"},{"subitem_subject":"Atropine","subitem_subject_scheme":"Other"},{"subitem_subject":"New internal surface reversed phase column","subitem_subject_scheme":"Other"},{"subitem_subject":"Shim-pack MAYI-ODS","subitem_subject_scheme":"Other"},{"subitem_subject":"LC/MS/MS","subitem_subject_scheme":"Other"}]},"item_language":{"attribute_name":"言語","attribute_value_mlt":[{"subitem_language":"eng"}]},"item_resource_type":{"attribute_name":"資源タイプ","attribute_value_mlt":[{"resourcetype":"journal article","resourceuri":"http://purl.org/coar/resource_type/c_6501"}]},"item_title":"LIQUID CHROMATOGRAPHIC / MASS SPECTROMETRIC DETERMINATION OF MORPHINE, CODEINE AND COCAINE IN HUMAN SERA USING A NEW INTERNAL SURFACE REVERSED PHASE COLUMN","item_titles":{"attribute_name":"タイトル","attribute_value_mlt":[{"subitem_title":"LIQUID CHROMATOGRAPHIC / MASS SPECTROMETRIC DETERMINATION OF MORPHINE, CODEINE AND COCAINE IN HUMAN SERA USING A NEW INTERNAL SURFACE REVERSED PHASE COLUMN","subitem_title_language":"en"}]},"item_type_id":"3","owner":"4","path":["11"],"pubdate":{"attribute_name":"PubDate","attribute_value":"2013-08-27"},"publish_date":"2013-08-27","publish_status":"0","recid":"1707","relation_version_is_last":true,"title":["LIQUID CHROMATOGRAPHIC / MASS SPECTROMETRIC DETERMINATION OF MORPHINE, CODEINE AND COCAINE IN HUMAN SERA USING A NEW INTERNAL SURFACE REVERSED PHASE COLUMN"],"weko_creator_id":"4","weko_shared_id":-1},"updated":"2023-08-02T04:00:48.807386+00:00"}