{"created":"2023-06-20T15:47:20.754046+00:00","id":1883,"links":{},"metadata":{"_buckets":{"deposit":"4be10f07-1360-4b92-9a17-1c0669f3c226"},"_deposit":{"created_by":4,"id":"1883","owners":[4],"pid":{"revision_id":0,"type":"depid","value":"1883"},"status":"published"},"_oai":{"id":"oai:hama-med.repo.nii.ac.jp:00001883","sets":["1:11"]},"author_link":["4845","4846","4847","4848","4849"],"item_3_biblio_info_5":{"attribute_name":"書誌情報","attribute_value_mlt":[{"bibliographicIssueDates":{"bibliographicIssueDate":"2009-09-28","bibliographicIssueDateType":"Issued"},"bibliographicIssueNumber":"1","bibliographicPageEnd":"84","bibliographicPageStart":"81","bibliographicVolumeNumber":"651","bibliographic_titles":[{"bibliographic_title":"Analytica Chimica Acta","bibliographic_titleLang":"en"}]}]},"item_3_description_9":{"attribute_name":"抄録","attribute_value_mlt":[{"subitem_description":"A rapid and sensitive electrospray ionization tandem mass spectrometric (ESI-MS-MS) procedure was developed for the determination of cyanide (CN-). CN- in biological fluids was reacted with NaAuCl4 to produce dicyanogold, Au(CN)2- which was extracted with methyl isobutyl ketone (MIBK). One μL of the extract was injected directly into an ESI-MS-MS instrument. Quantification of CN-was performed by selected reaction monitoring of the product ion CN- at m/z 26 that derived from precursor ion Au(CN)2- at m/z 249. CN- could be measured in the quantification range of 10-7 to 5×10-5 M with the limit of detection at 4×10-8 M using 10 μL of urine within 10 min. A victim’s urine and gastric content were diluted with water to 4-fold and 500-fold and measured, respectively.","subitem_description_language":"en","subitem_description_type":"Abstract"}]},"item_3_publisher_6":{"attribute_name":"出版者","attribute_value_mlt":[{"subitem_publisher":"Elsevier","subitem_publisher_language":"en"}]},"item_3_relation_28":{"attribute_name":"出版社DOI","attribute_value_mlt":[{"subitem_relation_type":"isVersionOf","subitem_relation_type_id":{"subitem_relation_type_id_text":"10.1016/j.aca.2009.08.001","subitem_relation_type_select":"DOI"}}]},"item_3_rights_7":{"attribute_name":"権利","attribute_value_mlt":[{"subitem_rights":"Copyright 2009 Elsevier B.V.","subitem_rights_language":"en"}]},"item_3_source_id_19":{"attribute_name":"ISSN","attribute_value_mlt":[{"subitem_source_identifier":"00032670","subitem_source_identifier_type":"ISSN"}]},"item_3_version_type_32":{"attribute_name":"著者版フラグ","attribute_value_mlt":[{"subitem_version_resource":"http://purl.org/coar/version/c_ab4af688f83e57aa","subitem_version_type":"AM"}]},"item_creator":{"attribute_name":"著者","attribute_type":"creator","attribute_value_mlt":[{"creatorNames":[{"creatorName":"Minakata, Kayoko","creatorNameLang":"en"}],"nameIdentifiers":[{"nameIdentifier":"4845","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"Nozawa, Hideki","creatorNameLang":"en"}],"nameIdentifiers":[{"nameIdentifier":"4846","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"Gonmori, Kunio","creatorNameLang":"en"}],"nameIdentifiers":[{"nameIdentifier":"4847","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"Suzuki, Masako","creatorNameLang":"en"}],"nameIdentifiers":[{"nameIdentifier":"4848","nameIdentifierScheme":"WEKO"}]},{"creatorNames":[{"creatorName":"Suzuki, Osamu","creatorNameLang":"en"}],"nameIdentifiers":[{"nameIdentifier":"4849","nameIdentifierScheme":"WEKO"}]}]},"item_files":{"attribute_name":"ファイル情報","attribute_type":"file","attribute_value_mlt":[{"accessrole":"open_date","date":[{"dateType":"Available","dateValue":"2018-08-27"}],"displaytype":"detail","filename":"ACA-651-81.pdf","filesize":[{"value":"254.9 kB"}],"format":"application/pdf","licensetype":"license_note","mimetype":"application/pdf","url":{"label":"ACA-651-81.pdf","url":"https://hama-med.repo.nii.ac.jp/record/1883/files/ACA-651-81.pdf"},"version_id":"048f027b-9434-4fbb-b59a-bc1cd0a1b7d5"}]},"item_keyword":{"attribute_name":"キーワード","attribute_value_mlt":[{"subitem_subject":"Cyanide","subitem_subject_language":"en","subitem_subject_scheme":"Other"},{"subitem_subject":"Gold","subitem_subject_language":"en","subitem_subject_scheme":"Other"},{"subitem_subject":"Electrospray ionization","subitem_subject_language":"en","subitem_subject_scheme":"Other"},{"subitem_subject":"Tandem mass spectrometry","subitem_subject_language":"en","subitem_subject_scheme":"Other"},{"subitem_subject":"Urine","subitem_subject_language":"en","subitem_subject_scheme":"Other"}]},"item_language":{"attribute_name":"言語","attribute_value_mlt":[{"subitem_language":"eng"}]},"item_resource_type":{"attribute_name":"資源タイプ","attribute_value_mlt":[{"resourcetype":"journal article","resourceuri":"http://purl.org/coar/resource_type/c_6501"}]},"item_title":"Determination of cyanide, in urine and gastric content, by electrospray ionization tandem mass spectrometry after direct flow injection of dicyanogold","item_titles":{"attribute_name":"タイトル","attribute_value_mlt":[{"subitem_title":"Determination of cyanide, in urine and gastric content, by electrospray ionization tandem mass spectrometry after direct flow injection of dicyanogold","subitem_title_language":"en"}]},"item_type_id":"3","owner":"4","path":["11"],"pubdate":{"attribute_name":"PubDate","attribute_value":"2013-08-27"},"publish_date":"2013-08-27","publish_status":"0","recid":"1883","relation_version_is_last":true,"title":["Determination of cyanide, in urine and gastric content, by electrospray ionization tandem mass spectrometry after direct flow injection of dicyanogold"],"weko_creator_id":"4","weko_shared_id":-1},"updated":"2023-08-02T02:08:40.529516+00:00"}