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局所麻酔薬8種のHPLC-MSによる分離分析法とSSI及びAPCI法の感度比較
http://hdl.handle.net/10271/1737
http://hdl.handle.net/10271/17372eebef9a-ea5c-439b-82a1-68cd3aeb9ab8
名前 / ファイル | ライセンス | アクション |
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FT-20-210.pdf (108.3 kB)
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Item type | 学術雑誌論文 / Journal Article(1) | |||||
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公開日 | 2013-08-27 | |||||
タイトル | ||||||
言語 | ja | |||||
タイトル | 局所麻酔薬8種のHPLC-MSによる分離分析法とSSI及びAPCI法の感度比較 | |||||
言語 | ||||||
言語 | jpn | |||||
資源タイプ | ||||||
資源タイプ識別子 | http://purl.org/coar/resource_type/c_6501 | |||||
資源タイプ | journal article | |||||
その他のタイトル | ||||||
その他のタイトル | SPARATION CONDITIONS AND COMPARISON OF SSI WITH APCI FOR EIGHT LOCAL ANESTHETICS BY HPLC-MS | |||||
言語 | en | |||||
著者 |
有信, 哲哉
× 有信, 哲哉× 服部, 秀樹× 岩井, 雅枝× 妹尾, 洋× 石井, 晃× 熊澤, 武志× 鈴木, 修 |
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書誌情報 |
ja : 法中毒 en : Japanese journal of forensic toxicology 巻 20, 号 2, p. 210-211, 発行日 2002-05-15 |
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出版者 | ||||||
言語 | ja | |||||
出版者 | 日本法中毒学会 | |||||
権利 | ||||||
言語 | ja | |||||
権利情報 | Copyright 日本法中毒学会 | |||||
権利 | ||||||
言語 | ja | |||||
権利情報 | 本文データは日本法中毒学会の許諾のもと掲載しています。 | |||||
抄録 | ||||||
内容記述タイプ | Abstract | |||||
内容記述 | We have developed a rapid determination method for local anesthetics of tetracaine, procaine, benzoxinate, dibucaine, lidocaine, bupivacaine and mepivacaine by high-performance liquid chromatography (HPLC)-mass spectrometry (MS) coupled with a diol-bonded silica gel HPLC column that enabled direct injection of biological samples. We have also compared the sensitivities for the drags by sonic spray ionization (SSI) and atmospheric pressure chemical ionization (APCI). Those by HPLC-SSI-MS for tetracaine, benzoxinate, dibucaine, bupivacaine and mepivacaine were 4, 16, 16, 8 and 4 times higher, respectively. Those by HPLC-SSI-MS for procaine and lidocaine were equivalent to those by HPLC-APCI-MS. From a synthetic view, the simultaneous analysis of local anesthetics by HPLC-SSI-MS seems to be better than HPLC-APCI-MS. | |||||
言語 | en | |||||
ISSN | ||||||
収録物識別子タイプ | ISSN | |||||
収録物識別子 | 09159606 | |||||
著者版フラグ | ||||||
出版タイプ | VoR | |||||
出版タイプResource | http://purl.org/coar/version/c_970fb48d4fbd8a85 |