| Item type |
学術雑誌論文 / Journal Article(1) |
| 公開日 |
2013-08-27 |
| タイトル |
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タイトル |
Simple Isotope Dilution Headspace-GC-MS Analysis of Naphthalene and p-Dichlorobenzene in Whole Blood and Urine |
|
言語 |
en |
| 言語 |
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|
言語 |
eng |
| 資源タイプ |
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資源タイプ識別子 |
http://purl.org/coar/resource_type/c_6501 |
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資源タイプ |
journal article |
| 著者 |
Watanabe, Kanako
Hasegawa, Koutaro
Yamagishi, Itaru
Nozawa, Hideki
Takaba, Masamitsu
Suzuki, Osamu
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| 書誌情報 |
en : Analytical Sciences
巻 25,
号 11,
p. 1301-1305,
発行日 2009-11-10
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| 出版者 |
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出版者 |
日本分析化学会 |
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言語 |
ja |
| 権利 |
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|
権利情報 |
Copyright The Japan Society for Analytical Chemistry |
| 権利 |
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|
権利情報 |
本文データは学協会の許諾に基づき社団法人日本分析化学会のホームページから複製したものである |
| 抄録 |
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内容記述タイプ |
Abstract |
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内容記述 |
A very simple and sensitive method for the simultaneous analysis of naphthalene and p-dichlorobenzene in human whole blood and urine by headspace capillary gas chromatography-mass spectrometry (GC-MS) is presented. The advantages of the method were that as much as 1 mL of headspace vapor could be injected into a GC port in the splitless mode, and that the addition of deuterated naphthalene and p-dichlorobenzene as internal standards resulted in much better headspace extraction efficiencies, which resulted in high sensitivity. The detection limits for both naphthalene and p-dichlorobenzene were 1 ng mL-1 for whole blood and 0.5 ng mL-1 for urine. Validation data, such as the linearity of calibration curves, reproducibility and recovery rates, were all satisfactory. Using this method, both compounds could actually be detected from whole blood samples of a male volunteer after the inhalation of each gas of the compounds. |
| ISSN |
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収録物識別子タイプ |
ISSN |
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収録物識別子 |
13482246 |
| 出版社DOI |
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関連タイプ |
isIdenticalTo |
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識別子タイプ |
DOI |
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関連識別子 |
10.2116/analsci.25.1301 |
| 著者版フラグ |
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出版タイプ |
VoR |
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出版タイプResource |
http://purl.org/coar/version/c_970fb48d4fbd8a85 |
a25_1301.pdf (370.6 kB)
