| Item type |
学術雑誌論文 / Journal Article(1) |
| 公開日 |
2013-08-27 |
| タイトル |
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|
タイトル |
ダイアジン系除草剤の固相抽出法とキャピラリーガスクロマトグラフィー |
|
言語 |
ja |
| 言語 |
|
|
言語 |
jpn |
| 資源タイプ |
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資源タイプ識別子 |
http://purl.org/coar/resource_type/c_6501 |
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資源タイプ |
journal article |
| その他のタイトル |
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その他のタイトル |
SOLID-PHASE EXTRACTION AND CAPILLARY GAS CHROMATOGRAPHY OF DIAZINE HERBICIDES |
| 著者 |
李, 暁鵬
熊澤, 武志
佐藤, 啓造
鈴木, 修
|
| 書誌情報 |
ja : 法中毒 = Japanese journal of forensic toxicology
巻 12,
号 2,
p. 118-119,
発行日 1994-05-20
|
| 出版者 |
|
|
出版者 |
日本法中毒学会 |
|
言語 |
ja |
| 権利 |
|
|
権利情報 |
Copyright 日本法中毒学会 |
| 権利 |
|
|
権利情報 |
本文データは日本法中毒学会の許諾のもと掲載しています。 |
| 抄録 |
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|
内容記述タイプ |
Abstract |
|
内容記述 |
A simple and rapid method, for the extraction of four diazine herbicides (terbacil, bromacil, norflurazon and PAC) from human whole blood, plasma and urine, using Bond-Elut C18 cartridges, is presented. After mixing with distilled water, whole blood, plasma and urine samples containing the herbicides were loaded on Bond-Elut C18 cartridges and eluted with chloroform/methanol(9:1). The herbicides were detected by capillary gas chromatography with flame ionization detection (FlD) with splitless injection. Separation of four diazine herbicides from each other and from impurities was generally satisfactory with the use of an intermediately polar DB-17 capillary column. The recovery of these compounds was more than 90%. The calibration curve for the four herbicides, which had been added to whole blood, plasma and urine, showed linearity in the range of 1.6-100 ng on column. The detection limits of the herbicides were about 1.2-1.4 ng on column. |
| ISSN |
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収録物識別子タイプ |
ISSN |
|
収録物識別子 |
09159606 |
| 著者版フラグ |
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出版タイプ |
VoR |
|
出版タイプResource |
http://purl.org/coar/version/c_970fb48d4fbd8a85 |
FT-12-118.pdf (122.5 kB)
