| Item type |
学術雑誌論文 / Journal Article(1) |
| 公開日 |
2013-08-27 |
| タイトル |
|
|
タイトル |
低温オーブントラッピングガスクロマトグラフィーによるヒト体液中スチレン及び関連物質の高感度分析 |
|
言語 |
ja |
| 言語 |
|
|
言語 |
jpn |
| 資源タイプ |
|
|
資源タイプ識別子 |
http://purl.org/coar/resource_type/c_6501 |
|
資源タイプ |
journal article |
| その他のタイトル |
|
|
その他のタイトル |
Sensitive determination of styrene and related compounds in human body fluids by headspace capillary gas chromatography with cryogenic oven trapping |
| 著者 |
渡部, 加奈子
鈴木, 修
石井, 晃
妹尾, 洋
鈴木, 加奈子
|
| 書誌情報 |
ja : 法中毒
en : Japanese journal of forensic toxicology
巻 19,
号 2,
p. 182-183,
発行日 2001-05-15
|
| 出版者 |
|
|
出版者 |
日本法中毒学会 |
|
言語 |
ja |
| 権利 |
|
|
権利情報 |
Copyright 日本法中毒学会 |
| 権利 |
|
|
権利情報 |
本文データは日本法中毒学会の許諾のもと掲載しています。 |
| 抄録 |
|
|
内容記述タイプ |
Abstract |
|
内容記述 |
A simple and sensitive method is presented for determination of styrene, toluene, ethylbenzene, isopropylbenzene and n-propylbenzene in human body fluids by capillary gas chromatography (GC) with cryogenic oven trapping. After heating a blood or urine sample containing each compound and p-diethylbenzene (IS) in a 7.0-ml vial at 60℃ for 20 min, 5 ml of the headspace vapor was drawn into a glass syringe and injected into a GC port. All vapor was introduced into an Rtx-Volatile middle bore capillary column in the splitless mode at 20℃ of oven temperature to trap entire analytes, and then the oven temperature was programmed up to 280℃ for GC measurements by with flame ionization detection. The present conditions gave sharp peaks of each compound and IS, and low background noises for whole blood or urine samples. Each compound could be determined for rat whole blood after inhalation of gas of the five compounds. The present GC with cryogenic oven trapping is recommendable for use in determinations of styrene and related compounds in forensic and environmental toxicology, because it is simple, requires no special GC operations and gives high sensitivity and good separations. |
| ISSN |
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|
収録物識別子タイプ |
ISSN |
|
収録物識別子 |
09159606 |
| 著者版フラグ |
|
|
出版タイプ |
VoR |
|
出版タイプResource |
http://purl.org/coar/version/c_970fb48d4fbd8a85 |
FT-19-182.pdf (144.7 kB)
