{"_buckets": {"deposit": "61a1a4c4-a9d8-4ce0-9f9f-c380ef8747b8"}, "_deposit": {"created_by": 4, "id": "2771", "owners": [4], "pid": {"revision_id": 0, "type": "depid", "value": "2771"}, "status": "published"}, "_oai": {"id": "oai:hama-med.repo.nii.ac.jp:00002771", "sets": ["11"]}, "author_link": [], "item_3_biblio_info_5": {"attribute_name": "書誌情報", "attribute_value_mlt": [{"bibliographicIssueDates": {"bibliographicIssueDate": "2012-07", "bibliographicIssueDateType": "Issued"}, "bibliographicIssueNumber": "2", "bibliographicPageEnd": "155", "bibliographicPageStart": "149", "bibliographicVolumeNumber": "30", "bibliographic_titles": [{"bibliographic_title": "Forensic Toxicology"}]}]}, "item_3_description_30": {"attribute_name": "フォーマット", "attribute_value_mlt": [{"subitem_description": "application/pdf", "subitem_description_type": "Other"}]}, "item_3_description_9": {"attribute_name": "抄録", "attribute_value_mlt": [{"subitem_description": "A rapid and sensitive mass spectrometric method was developed for the simultaneous determination of coinage metals such as copper (Cu), silver (Ag) and gold (Au). The metals in a wet ashed tissue solution were complexed with diethyldithiocarbamate (DDC; C4H10NCS2) and were extracted together with isoamyl alcohol. After the acidification of the extract with oxalic acid, metals were quantified using their product ions, Cu(DDCH)+, Ag(DDCH) + and Au(DDCH)+ that derived from the precursor ions Cu(DDC)2+, Ag(DDC)2 + and Au(DDC)2+, respectively, by electrospray ionization tandem mass spectrometry. The limits of detection were 0.6, 0.3 and 1 μgl?1 for Cu, Ag and Au and the quantification ranges were 2 ? 100, 1 ? 100 and 3 ? 100 μgl?1 for Cu, Ag and Au, respectively. Cu levels in spontaneously hypertensive osteogenic disorder rats at 6 weeks old and at 30 weeks old were found to be 1.8 times and 5.1 times those of the normotensive osteogenic disorder rats, respectively, when using wet-ashed kidney solutions diluted to 1,000 fold.", "subitem_description_type": "Abstract"}]}, "item_3_publisher_6": {"attribute_name": "出版者", "attribute_value_mlt": [{"subitem_publisher": "Springer Japan"}]}, "item_3_relation_28": {"attribute_name": "出版社DOI", "attribute_value_mlt": [{"subitem_relation_type": "isVersionOf", "subitem_relation_type_id": {"subitem_relation_type_id_text": "10.1007/s11419-012-0134-9", "subitem_relation_type_select": "DOI"}}]}, "item_3_rights_7": {"attribute_name": "権利", "attribute_value_mlt": [{"subitem_rights": "The final publication is available at Springer via http://dx.doi.org/10.1007/s11419-012-0134-9."}]}, "item_3_select_2": {"attribute_name": "資源タイプ", "attribute_value_mlt": [{"subitem_select_item": "Journal Article", "subitem_select_language": "en"}]}, "item_3_version_type_32": {"attribute_name": "著者版フラグ", "attribute_value_mlt": [{"subitem_version_resource": "http://purl.org/coar/version/c_ab4af688f83e57aa", "subitem_version_type": "AM"}]}, "item_creator": {"attribute_name": "著者", "attribute_type": "creator", "attribute_value_mlt": [{"creatorNames": [{"creatorName": "Minakata, Kayoko"}]}, {"creatorNames": [{"creatorName": "Yamagishi, Itaru"}]}, {"creatorNames": [{"creatorName": "Nozawa, Hideki"}]}, {"creatorNames": [{"creatorName": "Gonmori, Kunio"}]}, {"creatorNames": [{"creatorName": "Hasegawa, Koutaro"}]}, {"creatorNames": [{"creatorName": "Suzuki, Masako"}]}, {"creatorNames": [{"creatorName": "Horio, Fumihiko"}]}, {"creatorNames": [{"creatorName": "Watanabe, Kanako"}]}, {"creatorNames": [{"creatorName": "Suzuki, Osamu"}]}]}, "item_files": {"attribute_name": "ファイル情報", "attribute_type": "file", "attribute_value_mlt": [{"accessrole": "open_date", "date": [{"dateType": "Available", "dateValue": "2018-08-27"}], "displaytype": "detail", "download_preview_message": "", "file_order": 0, "filename": "ft-30-149.pdf", "filesize": [{"value": "7.2 MB"}], "format": "application/pdf", "future_date_message": "", "is_thumbnail": false, "licensetype": "license_note", "mimetype": "application/pdf", "size": 7200000.0, "url": {"label": "ft-30-149.pdf", "url": "https://hama-med.repo.nii.ac.jp/record/2771/files/ft-30-149.pdf"}, "version_id": "5343b2c9-5858-49a6-bec2-b368b3ca8665"}]}, "item_keyword": {"attribute_name": "キーワード", "attribute_value_mlt": [{"subitem_subject": "Copper", "subitem_subject_scheme": "Other"}, {"subitem_subject": "Silver", "subitem_subject_scheme": "Other"}, {"subitem_subject": "Gold", "subitem_subject_scheme": "Other"}, {"subitem_subject": "Electrospray ionization", "subitem_subject_scheme": "Other"}, {"subitem_subject": "Tandem mass spectrometry", "subitem_subject_scheme": "Other"}, {"subitem_subject": "Diethyldithiocarbamate", "subitem_subject_scheme": "Other"}]}, "item_language": {"attribute_name": "言語", "attribute_value_mlt": [{"subitem_language": "eng"}]}, "item_resource_type": {"attribute_name": "資源タイプ", "attribute_value_mlt": [{"resourcetype": "journal article", "resourceuri": "http://purl.org/coar/resource_type/c_6501"}]}, "item_title": "Simultaneous determination of coinage metals, copper, silver and gold in tissues using electrospray ionization tandem mass spectrometry", "item_titles": {"attribute_name": "タイトル", "attribute_value_mlt": [{"subitem_title": "Simultaneous determination of coinage metals, copper, silver and gold in tissues using electrospray ionization tandem mass spectrometry", "subitem_title_language": "en"}]}, "item_type_id": "3", "owner": "4", "path": ["11"], "permalink_uri": "http://hdl.handle.net/10271/2909", "pubdate": {"attribute_name": "PubDate", "attribute_value": "2015-11-20"}, "publish_date": "2015-11-20", "publish_status": "0", "recid": "2771", "relation": {}, "relation_version_is_last": true, "title": ["Simultaneous determination of coinage metals, copper, silver and gold in tissues using electrospray ionization tandem mass spectrometry"], "weko_shared_id": -1}
Simultaneous determination of coinage metals, copper, silver and gold in tissues using electrospray ionization tandem mass spectrometry
http://hdl.handle.net/10271/2909
http://hdl.handle.net/10271/2909